Manufacturing Technology 2023, 23(3):319-325 | DOI: 10.21062/mft.2023.045
Experimental Study on the Effect of Oxidation on the Compressibility of Iron Powder
- Department of Mechanical Engineering, Faculty of Engineering, Mutah University, Karak, Jordan
An experimental study was carried out on the effect of oxidation temperature and the oxide film composition on the compressibility of porous materials. samples were annealed at different temperatures; the size change in the samples after annealing was measured. The phase composition of the oxide layer was investigated. Magnetite was generated at between 350 and 450°C, and two-phase oxide was formed at 550°C, after oxidation, weight gain was determined. The presence of pore overgrowth, which reduces porosity, was confirmed by metallographic tests. The maximum porosity is found in the oxidized samples produced by pressing at room temperature. The process of high-temperature oxidation of iron powder before pressing and in the state of free filling in a fluidized bed, as well as the effect of the content of oxides on magnetic characteristics, has been studied. The impact of oxidation on the compressibility of samples of iron powder was investigated. In this study, It was observed that the range of 350-450°C, which offers the best compressibility and the necessary composition of the oxide film, is also related to the presence of magnetite in the iron oxide coating. is the ideal temperature for oxidation and repressing. the deformation of porous materials exposed to iron powder oxidation was tested.
Keywords: Oxidation, Iron powder, Soft magnetic materials, Deformation, Porous materials
Received: February 13, 2023; Revised: June 13, 2023; Accepted: June 22, 2023; Prepublished online: June 22, 2023; Published: July 5, 2023 Show citation
References
- PINGALE, Ajay D., et al. Recent research on Cu-Ni alloy matrix composites through electrodeposition and powder metallurgy methods: a review. Materials Today: Proceedings, 2021, 47: 3301-3308.
Go to original source...
- GONZALEZ-GUTIERREZ, Joamin, et al. Additive manufacturing of metallic and ceramic components by the material extrusion of highly-filled polymers: A review and future perspectives. Materials, 2018, 11.5: 840.
Go to original source...
- BRIKA, Salah Eddine, et al. Influence of particle morphology and size distribution on the powder flowability and laser powder bed fusion manufacturability of Ti-6Al-4V alloy. Additive Manufacturing, 2020, 31: 100929.
Go to original source...
- WEI, Chao, et al. Approaches for measuring the surface areas of metal oxide electrocatalysts for determining their intrinsic electrocatalytic activity. Chemical Society Reviews, 2019, 48.9: 2518-2534.
Go to original source...
- CORDOVA, Laura; CAMPOS, Mónica; TINGA, Tiedo. Revealing the effects of powder reuse for selective laser melting by powder characterization. Jom, 2019, 71.3: 1062-1072.
Go to original source...
- MARTÍN, Arturo; CEPEDA-JIMÉNEZ, Carmen María; PÉREZ-PRADO, María Teresa. Gas atomization of γ-TiAl Alloy Powder for Additive Manufacturing. Advanced Engineering Materials, 2020, 22.1: 1900594.
Go to original source...
- YODOSHI, Noriharu; ENDO, Takahide; MASAHASHI, Naoya. Evaluation of porosity in gas-atomized powder by synchrotron X-ray CT and investigation of the effect of gas species. Materials Transactions, 2021, MT-Y2021001.
Go to original source...
- SATHYAMOORTHY, G.; VIJAY, R.; LENIN SINGARAVELU, D. Brake friction composite materials: a review on classifications and influences of friction materials in braking performance with characterizations. Proceedings of the Institution of Mechanical Engineers, Part J: Journal of Engineering Tribology, 2022, 236.8: 1674-1706.
Go to original source...
- SINGH, D. Dev; MAHENDER, T.; REDDY, Avala Raji. Powder bed fusion process: A brief review. Materials Today: Proceedings, 2021, 46: 350-355.
Go to original source...
- LAMICHHANE, Tej Nath, et al. Additive manufacturing of soft magnets for electrical machines-A review. Materials Today Physics, 2020, 15: 100255.
Go to original source...
- BACK, J. A.; SCHAEFFER, L.; GAIO, J. C. Study of the electromagnetic properties of a soft magnetic composite (SMC) and its efficiency when applied to a low frequency magnetic field. Int J Eng, 2020, 9.6: 1-9.
- AHN, Byungmin. Recent advances in brazing fillers for joining dissimilar materials. Metals, 2021, 11.7: 1037.
Go to original source...
- IVANOV, Oleksandr, et al. Improvement of abrasion resistance of production equipment wear parts by hard facing with flux-cored wires containing boron carbide/metal powder reaction mixtures. Management Systems in Production Engineering, 2020.
Go to original source...
- THAKARE, Jayant Gopal, et al. Thermal barrier coatings-a state of the art review. Metals and Materials International, 2021, 27.7: 1947-1968.
Go to original source...
- MISHRA, Swayam Bikash, et al. Journey from 2D to 5D Printing: A Brief Review. Advances in Mechanical and Industrial Engineering, 2022, 95-101.
Go to original source...
- JULIEN, Paul C.; GRUBER, Robert J. Dry Toner Technology: 5.1 INTRODUCTION 5.1. 1 History of Xerography. In: Handbook of Imaging Materials. CRC Press, 2018. p. 191-226.
Go to original source...
- QIAN, Liwei, et al. Effect of annealing on magnetic properties of Fe/Fe3O4 soft magnetic composites prepared by in-situ oxidation and hydrogen reduction methods. Journal of Alloys and Compounds, 2019, 778: 712-720.
Go to original source...
- OH, Joo Won; SEONG, Yujin; PARK, Seong Jin. The effect of nanoparticles in bimodal powder on the physical and mechanical properties of powder injection molded parts. Journal of Materials Processing Technology, 2018, 262: 503-510.
Go to original source...
- CHOUDHURY, Nitamani; MEGHWAL, Murlidhar; DAS, Kalyan. Microencapsulation: An overview of concepts, methods, properties, and applications in foods. Food Frontiers, 2021, 2.4: 426-442.
Go to original source...
- DEEVI, Seetharama C. Advanced intermetallic iron aluminide coatings for high-temperature applications. Progress in Materials Science, 2021, 118: 100769.
Go to original source...
- XIAO B, ZHANG J, GENG L, TANG X, WANG Y, YIN T, ZHANG Y, GOU J, HE H. Studies on the influence of high-shear granulation process on the compressibility of microcrystalline cellulose. International Journal of Pharmaceutics. 2022 Sep 25;625:122075.
Go to original source...
- MIRAN HA, ALTARAWNEH M, WIDJAJA H, JAF ZN, RAHMAN MM, VEDER JP, DLUGOGORSKI BZ, JIANG ZT. Thermo-mechanical properties of cubic lanthanide oxides. Thin Solid Films. 2018 May 1;653:37-48.
Go to original source...
- REN P, LING TC, MO KH. Recent advances in artificial aggregate production. Journal of Cleaner Production. 2021 Apr 1;291:125215.
Go to original source...
- KADOTA K, TANAKA M, NISHIYAMA H, TSE JY, UCHIYAMA H, SHIRAKAWA Y, TOZUKA Y. An effective approach to modify the inhalable betamethasone powders based on morphology and surface control using a biosurfactant. Powder Technology. 2020 Oct 1;376:517-26.
Go to original source...
- SCHMELZER J. Microstructure and properties of powder metallurgical manufactured V-rich VSi-B al-loys for high-temperature application.
- RAMABULANA K. Sinterability Studies of High Carbon Steel Powders Containing Nickel, Molyb-denum, Cobalt and Manganese. University of Johannesburg (South Africa); 2020.
- spherical-ferromagnetic-iron-powder-7439-89-6_sds.pdf
- https://www.angstrom-advanced.com/pro2-2700.html
- LIPIŃSKI T. Influence of Impurity Morphology on the Fatigue Strength of High-Purity Structural Steel Melted in an Electric Furnace. Manufacturing Technology 2023, 23(1):53-59.
Go to original source...
- KOREČEK, D., SOLFRONK, P., SOBOTKA, J. (2022) Analysis of the Dual-phase Steel DP500 Stress-strain Characteristics During the Plane Shear Test, in Manufacturing Technology, Vol. 22, No. 1, doi:10.21062/mft.2022.015.
Go to original source...
- KUČEROVÁ, L., TICHÁ, I., STEHLÍK, A. (2021) Effect of Various Heat and Thermo-mechanical Treatments on Low Alloyed CMnAlNb High Strength Steel, in: Manufacturing Technology, Vol. 21, No. 6, pp. 824-828, doi: 10.21062/mft.2021.094.
Go to original source...
- KOREČEK, D., SOLFRONK, P., SOBOTKA, J. (2022) Analysis of the Dual-phase Steel DP500 Stress-strain Characteristics During the Plane Shear Test, in: Manufacturing Technology, Vol. 22, No. 1, doi:10.21062/mft.2022.015.
Go to original source...
- KUČEROVÁ, L., TICHÁ, I., STEHLÍK, A. (2021) Effect of Various Heat and Thermo-mechanical Treatments on Low Alloyed CMnAlNb High Strength Steel, in: Manufacturing Technology, Vol. 21, No. 6, pp. 824-828, doi: 10.21062/mft.2021.094.
Go to original source...
- MENDRICKY, R., SOBOTKA, J. (2020). Accuracy Comparison of the Optical 3D Scanner and CT Scanner. In: Manufacturing Technology. Vol. 20, No. 6, pp. 791-801. J. E. Purkyně University in Usti nad Labem, Czech Republic. ISSN 1213-2489.
Go to original source...
This is an open access article distributed under the terms of the Attribution-NonCommercial 4.0 International License (CC BY-NC 4.0), which permits non-comercial use, distribution, and reproduction in any medium, provided the original publication is properly cited. No use, distribution or reproduction is permitted which does not comply with these terms.