Manufacturing Technology 2015, 15(1):41-47 | DOI: 10.21062/ujep/x.2015/a/1213-2489/MT/15/1/41

Long-term Sub-zero Treatment of P/M Vanadis 6 Ledeburitic Tool Steel - a Preliminary Study

Peter Jurči1,*, Martin Kusý1, Jana Ptačinová1, Vladimír Kuracina1, Petra Priknerová2
1 Faculty of Material Sciences and Technology in Trnava, Paulínská 16, 917 24 Trnava, Slovakia
2 Prikner - tepelné zpracování kovů, Martínkovice 279, 550 01, Czech Republic, Priknerová Petra

The microstructure, the phase constitution and the tempering charts of Cr-V ledeburitic steel Vanadis 6 subjected to sub-zero treatment with various soaking times in liquid nitrogen have been investigated. The microstructures have been characterized using the light microscopy, scanning electron microscopy and X-ray diffraction. The hardness has been evaluated by Vickers method. The matrix is martensitic with certain amount of retained austenite, irrespectively to the time of sub-zero treatment. The amount of retained austenite, however, decreases up to the soaking time of 17 h and then remains almost constant. The microstructure of sub-zero treated steel contains enhanced portion of small globular carbides, as compared to conventionally heat treated material. These particles have a size of around 100 nm in most cases. The as-quenched hardness manifests a moderate increase due to the sub-zero treatment. The hardness decreases during subsequent tempering and this decrease is more pronounced in sub-zero treated samples.

Keywords: Cr-V ledeburitic steel, sub-zero treatment, retained austenite and martensite, carbides, hardness

Published: February 1, 2015  Show citation

ACS AIP APA ASA Harvard Chicago IEEE ISO690 MLA NLM Turabian Vancouver
Jurči P, Kusý M, Ptačinová J, Kuracina V, Priknerová P. Long-term Sub-zero Treatment of P/M Vanadis 6 Ledeburitic Tool Steel - a Preliminary Study. Manufacturing Technology. 2015;15(1):41-47. doi: 10.21062/ujep/x.2015/a/1213-2489/MT/15/1/41.
Download citation

References

  1. DAS, D., RAY, K.K., DUTTA, A.K. (2009). Influence of temperature of sub-zero treatments on the wear behaviour of die steel. Wear, Vol. 267, pp. 1361 - 1370. Go to original source...
  2. DAS, D., DUTTA, A.K., RAY, K.K. (2009). Influence of varied cryotreatment on the wear behaviour of AISI D2 steel. Wear, Vol. 266, pp. 297 - 309. Go to original source...
  3. DAS, D., DUTTA, A.K., RAY, K.K. (2010). Sub-zero treatments of AISI D2 steel: Part II. Wear behaviour. Mater. Sci. Engng., Vol. A527, pp. 2194 - 2206. Go to original source...
  4. DAS, D., DUTTA, A.K., RAY, K.K. (2009). Optimization of the duration of cryogenic processing to maximize wear resistance of AISI D2 steel. Cryogenics, Vol. 49, pp. 176 - 184. Go to original source...
  5. STRATTON, P.F. (2007). Optimising nano-carbide precipitation in tool steels. Mater. Sci. Engng., Vol. A449-451, pp. 809 - 812. Go to original source...
  6. MOHAN LAL, D., RENGANARAYANAN, S., KALANIHIDI, A. (2001). Cryogenic treatment to augment wear resistance of tool and die steels. Cryogenics, Vol. 41, pp. 149 - 155. Go to original source...
  7. AMINI, K., AKHBARIZADEH, A., JAVADPOUR, S. (2013). Investigating the effect of the quench environment on the final microstructure and wear behaviour of 1.2080 tool steel after deep cryogenic heat treatment. Mater. Design, Vol. 45, pp. 316 - 322. Go to original source...
  8. AKHBARIZADEH, A., AMINI, K., JAVADPOUR, S. (2012). Effects of applying an external magnetic field during the deep cryogenic heat treatment on the corrosion resistance and wear behaviour of 1.2080 tool steel. Mater. Design, Vol. 41, pp. 114 - 123. Go to original source...
  9. AMINI, K., AKHBARIZADEH, A., JAVADPOUR, S. (2012). Investigating the effect of holding duration on the microstructure of 1.2080 tool steel during the deep cryogenic treatment. Vacuum, Vol. 86, pp. 1534 - 1540. Go to original source...
  10. DAS, D., SARKAR, R., DUTTA, A.K., RAY, K.K. (2010). Influence of sub-zero treatments on fracture toughness of AISI D2 steel. Mater. Sci. Engng., Vol. A528, pp. 589 - 603. Go to original source...
  11. JURČI, P., ©U©TAR©IČ, B., LESKOV©EK, V. (2010). Fracture Characteristics of the Cr-V Ledeburitic Steel Vanadis 6. Materiali in Tehnologije/Materials and Technology, Vol. 44, pp. 79 - 86.
  12. BERNS, H. (1974). Restaustenit in ledeburitischen Chromstählen und seine Umwandlung durch Kaltumformen, Tiefkühlen und Anlassen. HTM, Vol. 29, pp. 236 - 247. Go to original source...
  13. PELLIZZARI, M., MOLINARI, A. (2002). Deep Cryogenic Treatment of Cold Work Tool Steel. In: Proc. of the 6th Int. Tooling Conf., (J. Bergstrom, G. Fredriksson, M. Johansson, O. Kotik, F. Thuvander (Ed.)), pp. 547 - 558, Karlstad University, Karlstad, Sweden.
  14. JURČI, P., SOBOTOVÁ, J., SALABOVÁ, P., PRIKNER, O., ©U©TAR©IČ, B., JENKO, D. (2013). Subzero treatment of P/M Vanadis 6 ledeburitic tool steel. Int. Heat Treatment and Surf. Engng., Vol. 7, pp. 125 - 128. Go to original source...
  15. TYSHCHENKO, A.I. THEISEN, W., OPPENKOWSKI, A., SIEBERT, S., RAZUMOV, O.N., SKOBLIK, A.P., SIROSH, V.A., PETROV, J.N., GAVRILJUK, V.G. (2010). Low-temperature martensitic transformation and deep cryogenic treatment of a tool steel. Mater. Sci. Engng., Vol. A527, pp. 7027 - 7039. Go to original source...
  16. COLLINS, D.N., DORMER, J. (1997). Deep Cryogenic Treatment of a D2 Cold-Work Tool Steel. Heat Treatment of Metals, Vol. 24, pp. 71 - 74.
  17. GAVRILJUK, V.G., THEISEN, W., SIROSH, V.V., POLSHIN, E.V., KORTMANN, A., MOGILNY, G.S., PETROV, J.N., TARUSIN, Y.V. (2013). Low-temperature martensitic transformation in tool steels in relation to their deep cryogenic treatment. Acta Mater., Vol. 61, pp. 1705 - 1715. Go to original source...
  18. DAS, D., RAY, K.K. (2012). Structure-property correlation of cub-zero treated AISI D2 steel. Mater. Sci. Engng., Vol. A541, pp. 45 - 60. Go to original source...
  19. DAS, D., DUTTA, A.K., RAY, K.K. (2010). Sub-zero treatments of AISI D2 steel: Part II. Wear behaviour. Mater. Sci. Engng., Vol. A527, pp. 2182 - 2193. Go to original source...
  20. BÍLEK, P., SOBOTOVÁ, J., JURČI, P. (2011). Evaluation of the Microstructural Changes in Cr-V Ledeburitic Tool Steel Depending on the Austenitization Temperature. Materiali in Tehnologije/Materials and Technology, Vol. 44, pp. 489 - 493.
  21. ASTM E975-13: Standard Practice for X-Ray Determination of Retained Austenite in Steel with Near Random Crystallographic Orientation, ASTM Book of Standards, vol. 3.01, West Conshohocken, PA, USA, 2004.
  22. SURBERG, C.H., STRATTON, P., LINGENHOELE, K. (2008). The effect of some heat treatment parameters on the dimensional stability of AISI D2. Cryogenics, Vol. 48, pp. 42 - 47. Go to original source...
  23. STOJKO, A. (2006). The Effect of Cryogenic Treatment on Structural and Phase Transformations in Iron-Carbon Martensite. PhD Thesis, Technical University of Denmark, Lyngby, Denmark.
  24. DAS, D., DUTTA, A.K., TOPPO, V., RAY, K.K.. (2007). Effect of Deep Cryogenic Treatment on the Carbide Precipitation and Tribological Behavior of D2 Steel. Mater. Manuf. Process, Vol. 22, pp. 474 - 480. Go to original source...
  25. COLLINS, D.N. (1996). Deep cryogenic treatment of tool steels-a review. Heat treatment of metals, Vol. 2, pp. 40-42.
  26. MENG, F., TAGASHIRA, K., AZUMA, R., SOHMA, H. (1994). Role of Eta-carbide Precipitation's in the Wear Resistance Improvements of Fe-12Cr-Mo-V-1.4C Tool Steel by Cryogenic Treatment. ISIJ Int., Vol. 34, pp. 205 - 210. Go to original source...
  27. AKHBARIZADEH, A., SHAFYEI, A., GOLOZAR, M.A. (2009). Effects of cryogenic treatment on wear behaviour of D6 tool steel. Mater. Des., Vol. 30, pp. 3259 - 3264. Go to original source...
  28. JURČI, P., KUSÝ, M., DOMÁNKOVÁ, M., ČAPLOVIČ, L., SOBOTOVÁ, J., SALABOVÁ, P., PRIKNER, O., JENKO, D. (2013). Tempering response of sub-zero procesed Cr-V ledeburitic steel Vanadis 6. In: Proc. of the 22nd Int. Conf. on Metallurgy and Materials (METAL) (TANGER s.r.o. (Ed.)), pp. 651 - 656, Tanger s.r.o., Brno, Czech Republic.