Manufacturing Technology 2016, 16(5):1157-1162 | DOI: 10.21062/ujep/x.2016/a/1213-2489/MT/16/5/1157

Testing of the New Chemical Pre-treatments Types Applied on the Steel Substrate

Jaroslava Svobodova, Pavel Kraus, Radek Lattner, Arlette Mrisova
Faculty of Production Technology and Management, J. E. Purkyne University in Usti nad Labem. Pasteurova 3334/7, 400 01 Usti nad Labem. Czech Republic

This article deals with the analysis of the chemical pre-treatment influence on the corrosion resistance of the low carbon unalloyed steel material after cold forming. These are the pre-treatments nanotechnology based. The layer is created by sol-gel technology. Except two used types of nano chemical pre-treatments is also used classical ferric phosphate. The six variants of chemical pre-treatments were prepared and these variants were then compared in terms of corrosion resistance and the way of exclusion and surface morphology using SEM and EDS analysis. The experimental samples were prepared for each variant. They were observed macroscopically and using SEM before corrosion load. These analysis shows the differences between each variant. Using SEM and EDS analysis was searched the typical elements for each variant and was observed the excluded layer and potential defects. The experimental samples were placed in the corrosion chamber and loaded according to the standard CSN EN ISO 9227 after this analyses. The surface of the experimental samples were without any other protection thus there was observed changes on the surface of the samples after one hour. The corrosion loading was finished after 24 hours. Experimental samples were evaluated macroscopically and were compared. The result of the experiment is the best variant of chemical pre-treatment in terms of corrosion protection of steel substrate concluded after all analyses and observations.

Keywords: Steel substrate, Chemical pre-treatment, Sol-gel, Nanotechnology, Corrosion

Published: October 1, 2016  Show citation

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Svobodova J, Kraus P, Lattner R, Mrisova A. Testing of the New Chemical Pre-treatments Types Applied on the Steel Substrate. Manufacturing Technology. 2016;16(5):1157-1162. doi: 10.21062/ujep/x.2016/a/1213-2489/MT/16/5/1157.
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References

  1. SVOBODOVÁ, J. (2014). Výzkum vlivu předúprav povrchů na bázi nanotechnologií na korozní odolnost lakovaného nízkouhlíkového nelegovaného ocelového materiálu. Ústí nad Labem: Univerzita J. E. Purkyně v Ústí nad Labem, Fakulta výrobních technologií a managementu, ISBN 978-80-7414-753-1.
  2. BRINKER, C., J., SCHERER, W. G. (1990). Sol-gel science: the physics and chemistry of sol-gel processing. Boston: Academic Press, ISBN 0121349705. Go to original source...
  3. PIERRE, A. C. (1998). Introduction to Sol-Gel Processing 2. Boston, USA, Kluwer Academic Publishers, 408 p., ISBN 978-0792381211. Go to original source...
  4. SCHUBERT, U., HÜSING, N. (2012). Synthesis of Inorganic Materials. VCH-Wiley Verlag GmbH, Weinheim, 3rd edn, ISBN 3-527-32714-1.
  5. HO©EK, J. (2010). Úvod do nanotechnologie. Praha: České vysoké učení technické, 2010. ISBN 978-80-01-04555-8.
  6. SVOBODOVA, J. (2014). SEM and EDS Analysis Used in Evaluation of Chemical Pre-treatment Based on Nanotechnology. Manufacturing Technology, Journal for Science, Research and Production, Vol. 14, No. 3, ISSN 1213-2489. Go to original source...
  7. SVOBODOVA, J., KRAUS, P., CAIS, J., LATTNER, R. (2016). Research of Chemical Pre-treatment Created by Sol-gel Process on the Polished Surface of Aluminium Substrate. Manufacturing Technology, Journal for Science, Research and Production, Vol. 16, No. 1, ISSN 1213-2489. Go to original source...
  8. SVOBODOVÁ, J., KRAUS, P. (2015). Hodnocení drsnosti a morfologie povrchu hliníkového plechu po aplikaci chemických předúprav na bázi nanotechnologií. Strojírenská technologie, ročník XX, číslo 2, s. 103-109, ISSN 1211-4162.
  9. SVOBODOVA, J, KRAUS, P (2015). Influence of Chemical Pre-treatments Nanotechnology Based Applied to the Al Sheet on the Roughness and Morphology of the Surface. Manufacturing Technology, Journal for Science, Research and Production, Vol. 15, No. 4, ISSN 1213-2489. Go to original source...