Manufacturing Technology 2019, 19(2):190-196 | DOI: 10.21062/ujep/268.2019/a/1213-2489/MT/19/2/190

Effect of Powder Recycling in Laser-based Powder Bed Fusion of Ti-6Al-4V

Lucia Denti1, Antonella Sola1, Silvio Defanti1, Corrado Sciancalepore2, Federica Bondioli3
1 Department of Engineering "Enzo Ferrari" (DIEF), University of Modena and Reggio Emilia, via P. Vivarelli 10, 41125 Modena. Italy
2 INSTM, Research Unit of Modena, Department of Engineering Enzo Ferrari (DIEF), University of Modena and Reggio Emilia, via P. Vivarelli 10, 41125 Modena. Italy
3 Department of Applied Science and Technology (DISAT), Polytechnic University of Turin, Corso Duca degli Abruzzi 24, 10129 Torino, Italy

Additive manufacturing (AM) has shown promise to process parts for end-use applications, however stringent requirements must be fulfilled in terms of reliability and predictability. The expensiveness of raw materials for AM, especially for metal-based Powder Bed Fusion (PBF), brings about the need for a careful recycling of powder, but the effect of powder reuse on both processing conditions and final part performance is still the focus of intensive research in the open literature. Although ASTM F2924-14 specifies the virgin-to-used powder ratio to be introduced to manufacture titanium-6aluminum-4vanadium (Ti-6Al-4V) components by PBF, a deeper understanding of the effect of powder recycling on the mechanical properties of finished parts is expected to foster a more efficient and safe reuse. The present contribution is therefore addressed to investigate the consequence of Ti-6Al-4V powder recycling on the flowability, particle size distribution and morphology of the feedstock material as well as on the density and tensile performance of built parts. In order to quantify the recyclability of powders, a new "average usage time" (AUT) parameter is defined to account for both the real usage time of the powder and the virgin-to-used powder mixing ratio. The new parameter, whose applicability can be readily extended to any kind of feedstock powder, offers a significant contribution to achieve a more consistent and economical recycling of raw materials for PBF processing.

Keywords: Laser-based powder bed fusion; Powder; Recycling; Ti6Al4V; Mechanical properties

Published: April 1, 2019  Show citation

ACS AIP APA ASA Harvard Chicago IEEE ISO690 MLA NLM Turabian Vancouver
Denti L, Sola A, Defanti S, Sciancalepore C, Bondioli F. Effect of Powder Recycling in Laser-based Powder Bed Fusion of Ti-6Al-4V. Manufacturing Technology. 2019;19(2):190-196. doi: 10.21062/ujep/268.2019/a/1213-2489/MT/19/2/190.
Download citation

References

  1. KRUTH, J.P., WANG, X., LAOUI, T., FROYEN, L. (2003). Lasers and materials in selective laser sintering. In: Assembly Autom, Vol. 23, pp. 357 - 371. Go to original source...
  2. TONG, J., BOWEN, C.R., PERSSON, J., PLUMMER, A. (2016). Mechanical properties of titanium-based Ti-6Al-4V alloys manufactured by powder bed additive manufacture. In: Mater Sci Tech, Vol. 33, pp. 11. Go to original source...
  3. FOUSOVÁ, M., VOJTĚCH, D., KUBÁSEK, J. (2016). Titanium alloy Ti-6Al-4V prepared by selective laser melting (SLM). In: Manufacturing Technology, Vol. 16, pp. 691 - 697. Go to original source...
  4. FOUSOVÁ, M., VOJTECH, D., (2017). Influence of process conditions on additive manufacture of Ti6Al4V alloy by SLM technology. In: Manufacturing Technology, Vol. 17, pp. 696 - 701. Go to original source...
  5. HANN, B. (2016). Powder reuse and its effects on Laser Based Powder Fusion Additive Manufactured Alloy 718. In: SAE Int J Aerosp, Vol. 9, pp. 209 - 213. Go to original source...
  6. SEIFI, M., SALEM, A., BEUTH, J., HARRYSSON, O., LEWANDOWSKI, J.J. (2016). Overview of materials qualification needs for metal additive manufacturing. In: JOM, Vol. 68, pp. 747 - 764. Go to original source...
  7. ASTM F2924-14, Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium with Powder Bed Fusion. (2014). ASTM International, West Conshohocken, PA.
  8. BRICÍN, D., KŘÍ®, A. (2018). Assessment of Usability of WC-Co Powder Mixtures for SLM. In: Manufacturing Technology, Vol. 18, 719 - 726. Go to original source...
  9. SEYDA, V., KAUFMANN, N., EMMELMANN, C. (2012). Investigation of aging processes of Ti-6Al-4V powder material in laser melting. In: Physics procedia of the 7th international conference & exhibition on photonic technologies LANE, vol. 39, Fürth, Germany, p. 425 - 431. Go to original source...
  10. TANG, H.P., QIAN, M., LIU, N., ZHANG, X.Z., YANG, G.Y., WANG, J. (2015). Effect of powder reuse times on additive manufacturing of Ti-6Al-4V by selective electron beam melting. In: JOM, Vol. 67, pp. 555 - 563. Go to original source...
  11. ASTM B822-17, Standard Test Method for Particle Size Distribution of Metal Powders and Related Compounds by Light Scattering. (2017). ASTM International, West Conshohocken, PA.
  12. ASTM B213-17, Standard Test Methods for Flow Rate of Metal Powders Using the Hall Flowmeter Funnel. (2017). ASTM International, West Conshohocken, PA.
  13. ASTM B964-16, Standard Test Methods for Flow Rate of Metal Powders Using the Carney Funnel. (2016). ASTM International, West Conshohocken, PA.
  14. ASTM D7891-15, Standard Test Method for Shear Testing of Powders Using the Freeman Technology FT4 Powder Rheometer Shear Cell. (2015). ASTM International, West Conshohocken, PA.
  15. EOS Titanium Ti64, Material Data Sheet, at: https://cdn.eos.info/a4eeb73865d54434/5926811b3739/Ti-Ti64_9011-0014_9011-0039_M290_Material_data_sheet_11-17_en.pdf; last accessed: May 31, 2018.
  16. ISO. Metallic Materials-Tensile Testing-Part 1: Method of Test at Room Temperature. (2016). UNI EN ISO 6892-1; International Organization for Standardization: Geneva, Switzerland.
  17. NOURI, A., SOLA, A. (2018). Metal particle shape: A practical perspective. In: Met Powder Rep, Vol. 73, pp. 276 - 282. Go to original source...
  18. JENIKE, A.W. Storage and flow of solids. (1964). In: Bulletin of the University of Utah 123, Vol. 53, pp. 207.
  19. ARDILA, L.C., GARCIANDIA, F., GONZÁLEZ DÍAZ, J.B., ÁLVAREZ, P., ECHEVERRIA, A., PETITE, M.M., DEFFLEY, R., OCHOA, J. Effect of IN718 recycled powder reuse on properties of parts manufactured by means of Selective Laser Melting. (2014). In: Physics procedia of the 8th international conference on photonic technologies LANE, vol. 56, Fürth, Germany, p. 99 - 107.
  20. SLOTWINSKI, J.A., GARBOCZI, E.J., STUTZMAN, P.E., FERRARIS, C.F., WATSON, S.S., PELTZ, M.A. Characterization of metal powders used for additive manufacturing. (2014). In: J Res Natl Inst Stand Technol, Vol. 119, pp. 460 - 493. Go to original source...
  21. ASM Aerospace Specification Metals Inc., available on-line at http://asm.matweb.com/search/SpecificMaterial.asp?bassnum=mtp641; last accessed: June 1, 2018.
  22. GONG, H., RAFI, K., GU, H., JANAKI RAM, G.D., STARR, T., STUCKER, B. Influence of defects on mechanical properties of Ti-6Al-4V components produced by selective laser melting and electron beam melting. (2015). In: Mater Des, Vol. 86, pp. 545 - 555. Go to original source...

This is an open access article distributed under the terms of the Attribution-NonCommercial 4.0 International License (CC BY-NC 4.0), which permits non-comercial use, distribution, and reproduction in any medium, provided the original publication is properly cited. No use, distribution or reproduction is permitted which does not comply with these terms.