Manufacturing Technology 2022, 22(2):185-191 | DOI: 10.21062/mft.2022.030

Microstructure and Mechanical Properties of 3D Printed Tool Steel after Various Precipitation Hardening Treatments

Ludmila Kučerová ORCID..., Karolína Burdová ORCID..., ©těpán Jeníček ORCID..., Julie Volkmannová ORCID...
Regional Technological Institute, University of West Bohemia, Univerzitní 8, 301 00 Pilsen, Czech Republic

Precipitation hardening is one of the most frequently used methods of the post-processing heat treatments of 3D printed tool steel 1.2709, as it increases the yield and ultimate tensile strengths of the steel. Within this work, the broad temperature range of 250°C – 550°C was tested with five differ-ent holds at each temperature to study the effect of processing parameters on the microstructure and mechanical properties. Maraging tool steel 1.2709 was produced by selective laser melting (SLM) technology and obtained results were compared with conventionally produced steel of the same chemical composition. Mechanical properties were established by hardness measurement and tensile test and the microstructure was characterised mainly by light and scanning electron microscopy. The peak hardening was for both steels reached after 6 hours of precipitation at 500 °C, however, apparent hardening effects of heat treatment were observed already after low-temperature heat treatments.

Keywords: Maraging steel, Selective laser melting, Additive manufacturing, Microstructure, Mechanical properties
Grants and funding:

The present contribution has been prepared under project ITI CZ.02.1.01/0.0/0.0/18_069/0010040, “Re-search of additive technologies for future application in mechanical engineering practice – RTI plus” under the auspices of the National Sustainability Programme I of the Ministry of Education of the Czech Republic aimed to support research, experimental development and innovation.

Received: August 30, 2021; Revised: May 3, 2022; Accepted: May 3, 2022; Prepublished online: May 3, 2022; Published: May 15, 2022  Show citation

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Kučerová L, Burdová K, Jeníček ©, Volkmannová J. Microstructure and Mechanical Properties of 3D Printed Tool Steel after Various Precipitation Hardening Treatments. Manufacturing Technology. 2022;22(2):185-191. doi: 10.21062/mft.2022.030.
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References

  1. TAN, Ch., ZHOUT, K., MA, W., et al. (2017) Microstructural evolution, nanoprecipitation behavior and mechanical properties of selective laser melted high-performance grade 300 maraging steel. In: Mater. Des. Vol. 134, pp. 23-34. ISSN 0264-1275. Go to original source...
  2. SONG, J., TANG, Q., FENG, Q., MA, S., SETCHI, R., YING, L., HAN, Q., FAN, X., ZHANG, M. (2019). Effect of heat treatment on microstructure and mechanical behaviours of 18Ni-300 maraging steel manufactured by selective laser melting. In: Optics & Laser Technology, Vol. 120, art. no. 105725. Elsevier Ltd. Netherlands. ISSN 0030-3992. Go to original source...
  3. MICHALCOVÁ, A., PALM, M., SENČEKOVÁ, L., ROLINK, WEISHEIT, A., KUBATÍK, T. F. (2015). Microstructures of Iron Aluminides Processed by Additive Layer Manufacturing and Spark Plasma Sintering. In: Manufacturing Technology, Vol. 15, No. 4, pp. 610 - 614. Manufacturing Technology - Engineering Science and Research Journal. Czech Republic. ISSN 1213-2489. Go to original source...
  4. FOUSOVÁ, M., DVORSKÝ, VOJTĚCH, D. (2017). Additively Manufactured Aluminium AlSi10Mg Al-loy. In: Manufacturing Technology, Vol. 17, No. 4, pp. 446 - 451. Manufacturing Technology - Engineering Science and Research Journal. Czech Republic. ISSN 1213-2489. Go to original source...
  5. BOURELL, D., KRUTH, J. P., LEU, M., LEVY, G., ROSEN, D., BEESE, A. M., CLARE, A. (2017). Materials for additive manufacturing. In: CIRP Annals, Vol. 66, No. 2, pp. 659-681. Elsevier Ltd. Nether-lands. ISSN 0007-8506. Go to original source...
  6. JÄGLE, E. A., SHENG, Z., WU, L., LU, L., RISSE, J., WEISHEIT, A., RAABE, D. (2016). Precipitation Reactions in Age-Hardenable Alloys During Laser Additive Manufacturing. In: JOM, Vol. 68, pp. 943-949. ISSN 1543-1851. Go to original source...
  7. DEHGAHI, S., GHONCHEH, M.H., HADADZADEH, A., SANJARI, M., AMIRKHIZ, B. S., MOHAMMADI, M. (2020). The role of titanium on the microstructure and mechanical properties of additively manufactured C300 maraging steels. In: Materials & Design, Vol. 194, art. no. 108965. Elsevier Ltd. Netherlands. ISSN 0264-1275. Go to original source...
  8. SHA, W., GUO, Z. (2009). Maraging steels: Modelling of microstructure, properties and applications, pp. 1 - 203. Woodhead Publishing, Belfast. ISBN 978-184569686-3
  9. CONDE, F.F., ESCOBAR, J.D., OLIVEIRA, J.P. JARDINI, A.L, BOSE FILHO W.W., AVILA J.A. (2019). Austenite reversion kinetics and stability during tempering of an additively manufactured maraging 300 steel. In: Additive Manufacturing, Vol. 29, art. no. 100804. Elsevier Ltd. Netherlands. ISSN 2214-8604. Go to original source...
  10. CASATI, R., LEMKE, J., VEDANI, M. (2017). Microstructural and Mechanical Properties of As Built, Solution Treated and Aged 18 Ni (300 grade) Maraging Steel Produced by Selective Laser Melting. In: La Metallurgia Italiana, Vol. 109, No. 1, pp. 11-20. Italy. ISSN 260843.
  11. JÄGLE, E. A., SHENG, Z., KÜRNSTEINER, P., OCYLOK, S., WEISHEIT A., RAABE, D. (2016). Comparison of Maraging Steel Micro- and Nanostructure Produced Conventionally and by Laser Additive Manufacturing. In: Materials, Vol. 10, pp. 1-15. Materials. MDPI. Switzerland. ISSN: 1996-1944. Go to original source...
  12. KUČEROVÁ, L., BURDOVÁ, K., JENÍČEK, ©., CHENA, I. (2021). Effect of solution annealing and precipitation hardening at 250 °C -550 °C on microstructure and mechanical properties of additively manufactured 1.2709 maraging steel. In: Materials Science and Engineering: Elsevier Ltd. Netherlands. ISSN: 0921-5093. Go to original source...
  13. KUČEROVÁ, L., ZETKOVÁ, I. (2016). Metallography of 3D printed 1.2709 tool steel. In: Manufacturing Technology, Vol. 16, No. 1, pp. 140 - 144. Manufacturing Technology - Engineering Science and Research Journal. Czech Republic. ISSN: 1213-2489. Go to original source...
  14. Electro Optical Systems, GmbH (2014). EOS MaragingSteel MS1/400W (2014)., online [2021-08-27], dostupné z: https://www.eos.info/03_system-related-assets/material-related-contents/metal-materials-and-examples/metal-material-datasheet/werkzeugstahl_ms1_cx/ms1/ms-ms1-m280_m290_400w_material_data_sheet_05-14_en.pdf
  15. KEMPEN, K., YASA, E., THIJS, L., KRUTH J.P., VAN HUMBEEK, J. (2011). Microstructure and mechanical properties of Selective Laser Melted 18Ni-300 steel. In: Physics Procedia, Vol. 12, No. 1, pp. 255-263. Elsevier Ltd. Netherlands. ISSN 1875-3892. Go to original source...
  16. KUČEROVÁ, L. ZETKOVÁ, I. JENÍČEK, ©. BURDOVÁ, K. (2021). Production of Hybrid Joints by Selective Laser Melting of Maraging Tool Steel 1.2709 on Conventionally Produced Parts of the Same Steel. In: Materials, Vol. 14, No. 9. MDPI. Switzerland. ISSN: 1996-1944. Go to original source...
  17. JÄGLE, E. A., CHOI, P.-P., VAN HUMBEECK, J., RAABE, D. (2014) Precipitation and austenite re-version behavior of a maraging steel produced by selective laser melting. In: J. Mater. Res., Vol. 29, pp. 2072-2079. ISSN 2044-5326. Go to original source...

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