Manufacturing Technology 2024, 24(2):255-264
The Manufacturing of Environmental Barrier Coatings by HV-APS Plasma Spraying Using Er2O3 and SiO2 Powder Mixture
- Research and Development Laboratory for Aerospace Materials, Rzeszow University of Technology, Powstancow Warszawy 12, 35-959 Rzeszow, Poland
Over the last decades, nickel-based superalloys with TBC coatings have been used as the main material for hot section turbine parts. The next step in the development of engines and increasing the combustion temperature is the use of Ceramic Matrix Composites (CMC). Nevertheless, in the presence of water vapour or molten salts, accelerated degradation of substrate material. This problems can be pre-vented by additional layers or coatings produced on its surface, or combinations of layers and coatings that form Environmental Barrier Coatings (EBCs). The aim of the research was the preparation of sam-ples of a mixture of erbium oxide powders with silicon oxide with the addition of: polyvinyl alcohol, starch and cellulose gum. Then their technological properties were examined. A mixture with the most favourable properties was selected and sprayed using HV-APS method using with various process parameters and investigated. Conducted research showed that energy of HV-APS process is too low for synthesis of erbium disilicate in the resulting coating. The material was only melted, not vaporized. Making powder agglomerates with an average size of 150 μm with the addition of 3% PVA leads to a significant decrease in the surface area of powder grains. This results in a significant increase in flowability and allows it to be used as a charge material for APS plasma spraying.
Keywords: Plasma spray, Environmental barrier coatings, EBC, TBC, HV-APS, Er2O3, SiO2
Received: October 31, 2023; Revised: March 15, 2024; Accepted: March 20, 2024; Prepublished online: March 20, 2024; Published: April 30, 2024 Show citation
References
- BELAN J, VAŠKO A, KUCHARIKOVÁ L, TILLOVÁ E, CHALUPOVÁ M. (2019), The SEM Metallography Analysis of Vacuum Cast ZhS6K Superalloy Turbine Blade after Various Working Hours. In: Manufacturing Technology.;19(5):727-733. doi: 10.21062/ujep/362.2019/a/1213-2489/MT/19/5/727.
Go to original source...
- MA, L.J., H. YU, X.H. MAO, C.R. LI, C.Y. FENG, F.N. LI. (2023). Influence of Cutting Tool and Drill-ing Process on the Machinability of Inconel 718. In: Manufacturing Technology, 23( 2): 204-215, DOI: 10.21062/mft.2023.013
Go to original source...
- JOPEK, J., MOKRZYCKA, M., GÓRAL, M., KOSCIELNIAK, B., OCHAL, K., DRAJEWICZ, M. (2023), High Temperature Protective Coatings for Aeroengine Applications. In: Manufacturing Technology, 23 (4), 436-448., DOI: 10.21062/mft.2023.052
Go to original source...
- CHOWDHURY, T.S., MOHSIN, F.T., TONNI, M.M., MITA, M.N.H., EHSAN, M.M., (2023), A critical review on gas turbine cooling performance and failure analysis of turbine blades, In: International Journal of Thermofluids, 18, 100329, https://doi.org/10.1016/j.ijft.2023.100329
Go to original source...
- KRBATA, M.; FABO, P.; KOHUTIAR, M.; ESCHEROVA, J.; KUBA, M.; KIANICOVA, M.; ECKERT, M., (2023), Possibilities of Using Impedance Spectroscopy for Indirect Measurements of Thin Layers of Al & Cr-Al Coatings on Ni-based Superalloy Inconel 713LC Applied by the "Out-of-pack" Dif-fusion Method. In: Manufacturing Technology 23 (3), 313-318, DOI: 10.21062/mft.2023.042
Go to original source...
- BARWINSKA, I., KOPEC, M., KUKLA, D., SENDEROWSKI, C., KOWALEWSKI, Z.L., (2023), Thermal Barrier Coatings for High-Temperature Performance of Nickel-Based Superalloys: A Synthetic Review, In: Coatings, 13 (4), 769, DOI: 10.3390/coatings13040769
Go to original source...
- GORAL, M., PYTEL, M., SOSNOWY, P., KOTOWSKI, S., DRAJEWICZ, M., (2013), Microstructural characterization of thermal barrier coatings deposited by APS and LPPS thin film methods, In: Solid State Phenomena, 197, 1-5, https://doi.org/10.4028/www.scientific.net/SSP.197.1
Go to original source...
- PĘDRAK, P., DRAJEWICZ, M., DYCHTOŃ, K., NOWOTNIK, A., (2016), Microstructure and thermal characteristics of SiC-Al2O3-Ni composite for high-temperature application, In: Journal of Thermal Analysis and Calorimetry, 125 ( 3), 1353-1356, https://doi.org/10.1007/s10973-016-5608-2
Go to original source...
- MOREL, C., BARANGER, E., LAMON, J., BRAUN, J., LORRETTE, C., (2023), The influence of internal defects on the mechanical behavior of filament wound SiC/SiC composite tubes under uniaxial tension, In: Journal of the European Ceramic Society, 435, 1797-1807, DOI10.1016/j.jeurceramsoc.2022.12.040
Go to original source...
- LÜ, X., LI, L., SUN, J., YANG, J., JIAO, J., (2023), Microstructure and tensile behavior of (BN/SiC)n coated SiC fibers and SiC/SiC minicomposites, In: Journal of the European Ceramic Society, 435, 1828-1842, DOI10.1016/j.jeurceramsoc.2022.12.032
Go to original source...
- ZOK, F.W., MAXWELL, P.T., KAWANISHI, K., CALLAWAY, E.B., (2020), Degradation of a SiC-SiC composite in water vapor environments, In: Journal of the American Ceramic Society, 1033, 1927-1941, https://doi.org/10.1111/jace.16838
Go to original source...
- FAUCETT, D.C., CHOI, S.R., (2011), In: Proceedings of the ASME Turbo Expo 1, 497-504, DOI 10.1115/GT2011-46771
Go to original source...
- MOKRZYCKA M., JOPEK J., SŁYŚ. A, GÓRAL M., OCHAŁ K., (2023), Modern materials used for environmental barrier coatings - a review, Ochrona Przed Korozją, 4, 104-112, DOI:10.15199/40.2023.4.2
Go to original source...
- LEE, K. N. (2015). Environmental Barrier Coatings for SiC/SiC. In: John Wiley and Sons
Go to original source...
- TEJERO-MARTIN, D.; BENNETT, C.; HUSSAIN, T. (2021) A review on environmental barrier coat-ings: History, current state of the art and future developments. In: Journal of the European Ceramic Society, 41, 1747-1768, https://doi.org/10.48550/arXiv.2007.14914
Go to original source...
- XU, J., SARIN, V., BASU, S., (2012), Stability study of EBC/TBC hybrid system on Si-based ceramics in gas turbines, In: Materials Research Society Symposium Proceedings, 1519, 21-27, DOI 10.1557/opl.2012.1717
Go to original source...
- RICHARDS, B. T.; WADLEY, H.N.G. (2014) Plasma spray deposition of tri-layer environmental barrier coatings. In: Journal of the European Ceramic Society, 34, 3069-3083, https://doi.org/10.1557/opl.2012.1717
Go to original source...
- GRACIA, E.; LEE, H.; SAMPATH, S. (2019) Phase and microstructure evolution in plasma sprayed Yb2Si2O7 coatings. Journal of the European Ceramic Society, 39, 1477-1486, https://doi.org/10.1016/j.jeurceramsoc.2018.11.018
Go to original source...
- RICHARDS, B. T.; SEHR, S.; DE FRANQUEVILLE, F.; BEGLEY, M. R.; WADLEY, H.N.G. (2016) Fracture mechanisms of ytterbium monosilicate environmental barrier coatings during cyclic thermal exposure. In: Acta Materialia, 103, 448-460, https://doi.org/10.1016/j.actamat.2015.10.019
Go to original source...
- RICHARDS, B. T.; BEGLEY, M. R.; WADLEY, H. N. G. (2015) Mechanisms of Ytterbium Monosili-cate/Mullite/Silicon Coating Failure During Thermal Cycling in Water Vapor. In: Journal of the American Ceramic Society, 98 (2), 4066-4075, DOI: 10.1111/jace.13792
Go to original source...
- TURCER, L.R., KRAUSE, A.R., GARCES, H.F., ZHANG, L., PADTURE, N.P., (2018), Environmen-tal-barrier coating ceramics for resistance against attack by molten calcia-magnesia-aluminosilicate (CMAS) glass: Part II, β-Yb2Si2O7 and β-Sc2Si2O7, In: Journal of the European Ceramic Society, 3811, 3914-3924, DOI 10.1016/j.jeurceramsoc.2018.03.010
Go to original source...
- PĘDRAK, P., DYCHTOŃ, K., DRAJEWICZ, M., GÓRAL, M., (2021), Synthesis of gd2zr2o7 coatings using the novel reactive ps-pvd process, In: Coatings, 1110, 1208, DOI 10.3390/coatings11101208
Go to original source...
- ROKICKI, P., GÓRAL, M., KUBASZEK, T., DYCHTON K., DRAJEWICZ M., WIERZBIŃSKA, M., OCHAL, K., (2022), The microstructure and thermal properties of Yb2SiO5 coating deposited using APS and PS-PVD methods, Archives of Materials Science and Engineering, 114, (2), 49-57, DOI10.5604/01.3001.0016.0025
Go to original source...
- KUBASZEK, T., NOWAK, W., PĘDRAK, P., TRYBUS, K., ŚLEMP, K. GÓRAL, M. (2019) "The formation of pyrochlores during plasma spraying of REO and zirconia oxides powder mixture", In: Jour-nal of Mechanical and Energy Engineering, 3 (2), 141-148. doi: 10.30464/jmee.2019.3.2.141.
Go to original source...
- PĘDRAK, P., GÓRAL, M., DYCHTON, K., WIERZBINSKA, M., KUBASZEK, T., (2022), The Influ-ence of Reactive PS-PVD Process Parameters on the Microstructure and Thermal Properties of Yb2 Zr2O7 Thermal Barrier Coating, In: Materials, 154, 1594, DOI 10.3390/ma15041594
Go to original source...
- KUBASZEK, T., GÓRAL, M., SŁYŚ, A., SZCZĘCH D., GANCARCZYK, K., DRAJEWICZ, M., The influence of HV-APS process parameters on microstructure and erosion resistance of metalloceramic WC-CrC-Ni coatings, In: Ceramics International, 49 (1),18007-18013, https://doi.org/10.1016/j.ceramint.2023.02.148
Go to original source...
- NOWAK W., KUBASZEK T., GÓRAL M., WIERZBA B., (2020), Durability of underaluminized thermal barrier coatings during exposure at high temperature, In: Surface and Coatings Technology, 382, 125236, https://doi.org/10.1016/j.surfcoat.2019.125236
Go to original source...
- DUDNIK, O.V., LAKIZA, S.M., GRECHANYUK, I.M., REDKO V.P., MAKUDERA A.A., GLABAY M.S., MAREK I.O, RUBAN, A.K., GRECHANYUK, M.I. (2021), Composite Ceramics for Thermal Barrier Coatings Produced From ZrO2 Doped with Yttrium-Subgroup Rare-Earth Metal Oxides, In: Pow-der Metallurgy and Metal Ceramics, 5911-12, 672-680, https://doi.org/10.1007/s11106-021-00202-8
Go to original source...
- WANG, Q., GUO, L., YAN, Z., YE, F., (2018), Phase composition, thermal conductivity, and toughness of TiO2-doped, Er2O3-stabilized ZrO2 for thermal barrier coating applications, In: Coatings, 8 (7), 253, https://doi.org/10.3390/coatings8070253
Go to original source...
- MIRANDA, F.S., CALIARI, F.R., CAMPOS, T.M., Leite, D.M.G., PESSOA R., ESSIPTCHOUK, A.M., PETRACONI, G., (2020) High-velocity plasma spray process using hybrid SiO2 + ZrO2 precursor for deposition of environmental barrier coatings, In: Surface and Coatings Technology, 404, art. no. 126447, https://doi.org/10.1016/j.surfcoat.2020.126447
Go to original source...
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